Posted: May 22nd, 2023

The process of synthesizing polysilane

The remaining residue that had very low boiling points (thus making them volatile) was then put under very low pressure. Finally twenty milliliters of THF was added to the resultant residue and the polymer was formed. The polymer was then taken through a gentle precipitation process by slowly adding it to seven hundred milliliters of ethanol. It was then frozen and dried and the polymers were formed as a yellow powder. As has been seen the synthesis of germole goes through the same process as that of silole. So anybody who wants to make germole only follows the same procedure but instead of silicone he or she should use germanium. The same procedure is also followed when making silole-germole polymers (Cornils 618).

The process of synthesizing polysilane is as illustrated below

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